Sequence #2



Files

Athena project

Fe_Wustite-02.prj

XAS scans

Motor positions

XAFS stages:
xafs_x, 133.240
xafs_y, 112.312
xafs_pitch, -0.725
xafs_roll, 0.400
xafs_wheel, -30.000
xafs_ref, -75.000
xafs_refx, -77.400
xafs_refy, -4.221
xafs_det, 205.000
xafs_garot, 0.000
Instruments:
slot, 1.000
spinner, 1.000
dm3_bct, 43.702
Slits3:
slits3_vsize, 1.000
slits3_vcenter, 0.000
slits3_hsize, 5.000
slits3_hcenter, -0.201
slits3_top, 0.500
slits3_bottom, -0.500
slits3_inboard, -2.700
slits3_outboard, 2.299
M2:
m2_vertical, 6.000
m2_lateral, -0.001
m2_pitch, -0.000
m2_roll, 0.001
m2_yaw, 0.204
m2_yu, 6.000
m2_ydo, 6.000
m2_ydi, 6.000
m2_xu, -0.132
m2_xd, 0.131
m2_bender, 107241.000
M3 (Si stripe):
m3_vertical, 0.000
m3_lateral, -8.000
m3_pitch, 3.500
m3_roll, 0.000
m3_yaw, -0.000
m3_yu, -1.167
m3_ydo, 1.167
m3_ydi, 1.167
m3_xu, -8.000
m3_xd, -8.000
XAFS table:
xt_vertical, 129.878
xt_pitch, 4.866
xt_roll, 0.000
xt_yu, 127.056
xt_ydo, 132.701
xt_ydi, 132.701
Slits2:
slits2_vsize, 1.100
slits2_vcenter, 0.721
slits2_hsize, 18.005
slits2_hcenter, 0.697
slits2_top, 1.271
slits2_bottom, 0.171
slits2_inboard, -8.305
slits2_outboard, 9.699
Diagnostics:
dm3_foils, -2.749
dm2_fs, 34.058

Sample details

  • Sample composition: FeO
  • Sample preparation: powder on tape
  • Comment: Welcome to BMM

Instrument: Ex situ sample wheel

  • Slot number: 1
  • Ring: outer

Snapshots

  • Rough, automated data reduction
  • Image from XAS web camera     (uid)
  • Image from analog pinhole camera     (uid)
  • Image from USB camera #1     (uid)
  • Image from USB camera #2     (uid)

Scan details

  • E0: 7112.0 eV
  • Element: Fe (Iron, 26)
  • Edge: K
  • Mode: transmission
  • Bounds: -200.0 -30.0 -10.0 25.0 12k
  • Steps: 10.0 2.0 0.3 0.05k
  • Times: 0.5 0.5 0.5 0.5
  • Reference: Fe foil

Experiment configuration

  • Sequence start time: Thursday, October 12, 2023 02:16 PM
  • Sequence end time: Thursday, October 12, 2023 02:23 PM
  • Monochromator: Si(111)
  • Photon delivery mode: E (unfocused, 6 to 8 keV)
  • Pseudo-channel-cut energy: 7266.3 eV
  • Experimenters: XAS School 2023
  • General user proposal (GUP): 313917
  • Safety approval form (SAF): 312411